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  1. 防災科研関係論文

ガラスビードを用いた蛍光X線分析装置による珪酸塩岩石の主・微量成分分析:3倍・6倍・11倍希釈ガラスビード法の分析精度の評価

https://nied-repo.bosai.go.jp/records/3378
https://nied-repo.bosai.go.jp/records/3378
325d042a-0fe8-4cf2-b4c7-dee99cc4303f
Item type researchmap(1)
公開日 2023-03-30
タイトル
言語 ja
タイトル ガラスビードを用いた蛍光X線分析装置による珪酸塩岩石の主・微量成分分析:3倍・6倍・11倍希釈ガラスビード法の分析精度の評価
タイトル
言語 en
タイトル Major and Trace Components Analysis of Silicate Rocks by X-ray Fluorescence Spectrometer Using Fused Glass Beads : Evaluation of Analytical Precision of Three, Six, Eleven Times Dilution Fused Glass Beads Methods
言語
言語 jpn
著者 谷 健一郎

× 谷 健一郎

ja 谷 健一郎

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折橋 裕二

× 折橋 裕二

ja 折橋 裕二

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中田 節也

× 中田 節也

ja 中田 節也

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抄録
内容記述タイプ Other
内容記述 <論説>
言語 ja
抄録
内容記述タイプ Other
内容記述 We established a quantitative analysis for 10 major and 15 trace elements in silicate rocks by X-ray fluorescence spectrometry (XRF), using three types of dilution ratio glass bead, i.e., sample : flux ratios of 1 : 2, 1 : 5 and 1 : 10. The individual calibration lines, constructed using 24 igneous rock reference materials issued by USGS and GSJ, showed excellent accuracy and correlation coefficient for both major and trace elements, and no difference among the three types of glass beads, but, overall, the low dilution glass bead method (1 : 2) presented good analytical precision of both major and trace element in comparison with the other high dilution glass beads (1 : 5 and 1 : 10). For the assessment of our data quality, five reference rock materials of SY-2, SY-3, MRG-1, MIN-L and NIM-G, issued by SABS and CANMET were measured using above low dilution glass bead method. Our results were in good agreement with the recommended values reported by Potts et al. (1992), excluding Nb in SY-2, Co, Cr and Rb in SY-3, Ba and Pb in MRG-1, and Co and Ni in NIM-G. This suggests that our XRF method using low dilution glass bead is suitable to rapid and accurate determination of major and trace elements in silicate rocks from single glass bead.
言語 en
書誌情報 ja : 地震研究所技術研究報告

巻 8, 号 8, p. 26-36, 発行日 2002
出版者
言語 ja
出版者 東京大学地震研究所
ISSN
収録物識別子タイプ ISSN
収録物識別子 1342-6486
DOI
関連識別子 10.15083/00032214
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